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A technique for real-time detecting, locating,
and quantifying damage in large polymer
composite structures made of...
Article in Structural Health Monitoring · January 2015
DOI: 10.1177/1475921714546063
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Original Article
A technique for real-time detecting,
locating, and quantifying damage in
large polymer composite structures
made of carbon fibers and carbon
nanotube networks
Structural Health Monitoring
2015, Vol. 14(1) 35–45
Ó The Author(s) 2014
Reprints and permissions:
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DOI: 10.1177/1475921714546063
shm.sagepub.com
Ali Naghashpour1,2 and Suong Van Hoa1,2
Abstract
A significant safety concern preventing extensive use of composite materials for large polymer composite structures is
the ability to detect, locate, and quantify damages that occur at one or several locations in large polymer composite
structures. Real-time health monitoring of large polymer composite structures improves their performance, durability,
and reliability while minimizing the life cycle cost. In this article, we present a new, practical, and real-time structural
health monitoring technique for detecting, locating, and quantifying damages in large polymer composite structures made
of carbon fibers and carbon nanotube networks. In this technique, electrically conductive epoxy resin was prepared by
dispersing multiwalled carbon nanotubes into epoxy matrix. This modified epoxy matrix was then incorporated with
long carbon fibers to make large composite plates. Two sets of grid points made from silver-epoxy paste were mounted
on the surface of the large plates. The first set was used to apply the constant electric current, and the second set was
utilized to measure the electric potential. The electric potentials across the second set of grid points on the undamaged
plate were measured and used as a reference set. Two different damages were created by drilling holes and by applying
impact loading on the large plates. It is found that the electric potential between the contact points surrounding the
damage changes. The significant change in electric potential corresponds to the damage location in the plates. As such,
drilled holes, impact damages, and barely visible impact damages are detected, located, and quantified.
Keywords
Damage location, damage detection, carbon nanotubes, large polymer matrix composite structures, electrical properties
Introduction
Carbon fiber–reinforced polymer composites (CFRPCs)
have received attention in many industrial applications
due to their high strength-to-weight and stiffness-toweight ratios. One of the critical challenges in the practical use of CFRPCs is to monitor the health of large
polymer composite structures (LPCSs) in real time due
to their susceptibility to different types of damages.1
The long-term use of the composites depends on the
ability to detect and locate the damages in the structures. Various non-destructive evaluation (NDE)
techniques such as X-ray tomography,2,3 ultrasonic
C-scanning,2,4 liquid penetrant,2,5 acoustic emission,2,4,6
piezoelectric active sensors,2,7 fiber optics,2,4,8 and measuring electrical conductivity along the direction of carbon fibers2,9 have been used for detecting damage in
CFRPC structures. Techniques such as liquid penetrant,
ultrasound scanning, and X-ray can detect damages in
composites, but these techniques can only work in a
laboratory setting. They cannot be used on real composite structures during the operation of the engineering
component. Techniques such as acoustic emission can
1
Concordia Centre for Composites (CONCOM), Department of
Mechanical & Industrial Engineering, Concordia University, Montreal,
QC, Canada
2
Center for Applied Research on Polymers and Composites (CREPEC),
Montreal, QC, Canada
Corresponding author:
Ali Naghashpour, Concordia Centre for Composites (CONCOM),
Department of Mechanical & Industrial Engineering, Concordia University,
1455 De Maisonneuve Blvd. W., Montreal, QC H3G 1M8, Canada.
Email: al_nag@encs.concordia.ca
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36
Structural Health Monitoring 14(1)
detect the occurrence of damage in composite structures.
However, it is very difficult for this technique to locate
the damage due to confusion created by extraneous
sources. Techniques such as the use of fiber optical sensors can measure strains in the composite structures.
The optical fibers may pick up the change in strains due
to the occurrence of defects. However, the diameter of
the optical fiber is large (52 mm, which is more than six
times the diameter of a carbon fiber). When the optical
fibers are incorporated within the composite structures,
they create stress concentration that can degrade the
mechanical properties of the composite structures.
Besides, the optical fibers are fragile and tend to break
fairly easily.9,10 Over the past few years, measuring the
electrical conductivity of the carbon fibers was used as a
technique to indicate the presence of damage by many
researchers.11–24 Since carbon fibers are electrically conductive along the fiber direction, by applying an electric
current over two probes at two points along the direction of the fibers, the change in electric potential can be
taken as an indication of damage in CFRPC structures.
Schulte and Baron11 first proposed electrical resistance
change measurement (ERCM) for structural health
monitoring (SHM), which can be used to monitor the
internal damage of CFRPCs. Wang et al.20,21 showed
that the electric potential change measurement (EPCM)
is more sensitive than ERCM to detect internal damage
in CFRPC plates where the electric potential probes are
close to the electric current probes (current input locations). The problem with this technique is that since the
resin is not conductive, one cannot use the technique to
detect resin cracks. The majority of damage at the relatively low loads is due to matrix cracking and delamination, rather than fiber breakage. As such, the usefulness
of this technique is limited. Recent advent of polymer
nanocomposites in which carbon nanotubes (CNTs) are
added in polymers has provided the impetus for scientists and researchers in producing functionally tailored
matrix and fibers. This is because CNTs possess outstanding properties, including structural, mechanical,
electrical, and thermal properties.25 The outstanding
properties of CNTs combined with their small size offer
the potential to not only modify polymers but also
detect both strain and subsequently failure in polymer
matrix composites (PMCs). Adding CNTs at small concentrations in a polymer matrix to form electrically conductive networks distributed around the structural fiber
reinforcement displays piezoresistive behavior. The
piezoresistive behavior of the CNT networks enables
their use as highly responsive sensors to monitor initiation and detection of matrix cracks in the structures.26–
28
Zhang et al.29 embedded CNTs in graphite fiber/
epoxy laminates to improve their electrical conductivity
in the thickness direction due to continuous electrical
conduction pathways made by CNTs in between
graphite fibers. This approach was used to detect delamination created by inserting a Teflon film in the laminates. They found that there is a good correspondence
between the delamination length and changes in
through-thickness electrical resistance. Kostopoulos et
al.30 dispersed CNTs in carbon fiber/epoxy composite
not only for improving the electrical conductivity of the
composite in transverse direction but also for detecting
matrix cracks in the composite. They found that the
addition of CNTs in the composites acts as direct sensors with high damage sensitivity to detect matrix damage accumulation during monotonic and cyclic tensile
loading. The above works illustrate very interesting
and innovative attempts to monitor damage in
CFRPC coupons with small size using CNT networks.
No technique has existed to detect and locate damage
in LPCSs made of carbon fibers and CNT networks.
Here, we provide a technique to detect, locate, and
quantify damage in large carbon fiber/epoxy/CNT
composite plates.
Experimental methods
Materials
Multiwalled carbon nanotubes (MWCNTs) with 95%
purity, diameters of 2–20 nm, and lengths of 1 mm to
more than 10 mm were purchased from Bayer
MaterialScience. Plain weave woven carbon fabric
(5.7 oz/yd2) purchased from US Composites, Inc. with
thickness of 0.01 in, Epon 862 and EPIKURE W purchased from Miller-Stephenson Chemical Company
were utilized as reinforcement, epoxy resin, and curing
agent, respectively.
Methods
Fabrication of composite plates. To manufacture the carbon fiber/epoxy/MWCNT composite plates, 0.3 wt%
MWCNT (as the optimal quantity of MWCNT)27 was
dispersed into epoxy resin mixed with curing agent
(26.4 wt%) using three-roll milling (EXAKT 80E;
EXAKT Technologies, Inc.). The mixture was heated
up to 60°C for 20 min in a vacuum oven to remove air
bubbles. The modified epoxy matrix was dispersed in
six layers of plain weave carbon fabric by hand layup.
The composite plates were cured using an autoclave.
Electrical measurement strategy. Electrical measurement
can be performed by two methods for detecting damage in composite structures. One is a two-probe method
and the other is a four-probe method. In the two-probe
method, two electrical contacts are used to apply constant electric voltage and to determine electrical resistance based on the measured electric current. In the
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37
Naghashpour and Hoa
Figure 1. Schematic illustrating the strategy for EPM using the four-probe method.
EPM: electric potential measurement.
four-probe method, four electrical contacts are used.
One pair of electrical contacts is utilized to apply constant electric current between the two probes, while the
other pair is used to measure electric potential over two
points in the vicinity of the first two points. Contact
resistance exists between the probes and the plate. In
situations where the intrinsic resistance of the material
is much larger than the contact resistance at the probes
(such as glass fiber/epoxy composites containing CNT),
the effect of the contact resistance is small and the twoprobe method can be used effectively. However, in
situations where the intrinsic resistance of the material
is small compared to the contact resistance at the
probes (such as the case of carbon fiber/epoxy composites containing CNT), contact resistance is more dominant and the two-probe method is not suitable. In this
case, four-probe method is more suitable since electric
potential does not depend on the contact resistance at
the probes. Wang et al.22 demonstrated that four-probe
method is very effective and accurate compared to twoprobe method for detecting damage in CFRPC structures. As such, in this work, four-probe method is used
to minimize contact resistance. Another issue in using
electrical method for damage detection in twodimensional plate is current spreading that reduces
damage sensitivity. High sensitivity for detection of
minor damage in the structures can be achieved where
current input location is close to the electric potential
line.20,21 This close distance between electric current
line and electric potential line provides high current
density while minimizing current spreading. A new
strategy for electric potential measurement (EPM) is
proposed to overcome the aforementioned issues for in
situ damage monitoring in LPCSs made of carbon
fibers and CNT networks. The EPM strategy is
described in Figure 1. In this figure, two sets of grid
points are applied to avoid the contact resistance issue.
The first set is used to inject constant electric current
by pairs of I1I,2I, I1I,3I, I2I,4I, I3I,4I, I2I,3I, and I1I,4I (not
shown for clarity). The second set is utilized to measure
electric potentials between adjacent pairs of V1V,2V,
V1V,3V, V2V,4V, V3V,4V,V2V,3V, and V1V,4V (not shown
for clarity), where I and V stand for electric current
and potential. The subscript numbers, separated by a
space, represent the associated first and second sets of
grid points, respectively.
Composite plate specification and electrical measurement
strategy. The specification of composite plate and a new
strategy for EPM for in-situ damage monitoring are
schematically illustrated in Figure 2. In this figure, two
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38
Structural Health Monitoring 14(1)
Figure 2. Schematic illustration of composite plate specification and strategy for EPM.
EPM: electric potential measurement.
sets of grid points were mounted on the surface of
CFRPC structures. Each set consists of 40 electrical
contact points. Each contact point was made from electrically conductive silver-epoxy paste. The first set of
grid points labeled from 1I to 40I spaced 3 in apart was
used to apply a constant electric current to CFRPC
structures. The second set of grid points labeled from
1V to 40V spaced 3 in apart was diagonally shifted by
0.2 in with respect to the first set to measure electric
potentials. Electrical wires were attached to the two
grid points to make electrodes. Then, the electrodes
were connected to the data acquisition system (Vishay
Micro-Measurements System 7000) and a computer
with program.
The EPM strategy corresponding to nearest points
13I and 13V is described in Figure 3. In this figure, the
pairs of first set of grid points corresponding to point
13I identified by solid red lines to inject constant electric current are I13I,7I, I13I,8I, I13I,9I, I13I,12I, I13I,14I,
I13I,17I, I13I,18I, and I13I,19I, while the pairs of second set
of grid points corresponding to point 13V identified by
dashed blue lines to measure electric potentials are
V13V,7V, V13V,8V, V13V,9V, V13V,12V, V13V,14V, V13V,17V,
V13V,18V, and V13V,19V.
The current input location to measure electric
potential between one point and its nearest neighbors
(e.g. for points 13I and 13V) is presented in Table 1.
In this table, for example, constant electric current is
injected between points 13 and 7 (I13I,7I), while electric potential is measured between points 13 and 7
(V13V,7V). Another example is to inject constant electric current between points 13 and 8 (I13I,8I) while
measuring electric potential between points 13 and 8
(V13V,8V).
Electric potential measurement. The EPM is used to
detect damage in carbon fiber/epoxy/MWCNT composite plates. The EPM adopts the electrically conductive
carbon fibers and CNTs themselves as self-sensing
materials. The EPM was performed by four-probe
method using Keithley 6220 DC, Keithley 218A, and
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39
Naghashpour and Hoa
Drilled holes and impact tests
Two damage types were introduced in carbon fiber/
epoxy/MWCNT composite plates. One was drilled
holes of different sizes at different locations in the
plates. The other was impact damages caused by collision with high-velocity projectiles and drop weights on
the plates. The plates were subjected to high-velocity
impacts with energy of 78 J produced by a 318 mg aluminum particle traveling at 700 m/s using a gas gun.
The details of high-velocity impact test set-up to detect
and locate damage are shown in Figure 4. The drop
weights were applied on the clamped plates placed on
electrically non-conductive rigid supports to create the
low-velocity impacts.
Result and discussion
Figure 3. Schematic illustration for describing pairs of
electrical contacts corresponding to points 13I and 13V to inject
constant electric current (solid red lines) and to measure
electric potentials (dashed blue lines).
Table 1. Pairs of electrical contacts nearest to points 13I and
13V.
Pairs of electrical
contacts
Constant current
input location
Measured electric
potential
13–7
13–8
13–9
13–12
13–14
13–17
13–18
13–19
I13I,7I
I13I,8I
I13I,9I
I13I,12I
I13I,14I
I13I,17I
I13I,18I
I13I,19I
V13V,7V
V13V,8V
V13V,9V
V13V,12V
V13V,14V
V13V,17V
V13V,18V
V13V,19V
Vishay Micro-Measurements System 7000. A constant
current (100 mA) was directly applied by the mounted
first grid points through the plate using Keithley 6220
DC. Then, the electric potential across the second grid
points was measured using Keithley 218A. Electric
potential change (EPC) is expressed as
DV (%) =
Vf, iv, jv VI, iv, jv
3100
VI, iv, jv
ð1Þ
where VI, iv, jv and Vf, iv, jv represent the initial and final
electric potential values between grid points iv and jv,
respectively.
The electric potential values between pairs of second
set of grid points spaced 3 in apart before damage for
22 3 13 in2 carbon fiber/epoxy/0.3 wt% MWCNT
composite plate 1 were measured and used as reference
values. The electric potential distribution of plate 1 is
shown in Figure 5(a). Coefficient of variation in percent (100 3 standard deviation divided by average electric potential) as a measure of uniformity of electric
potential distribution for carbon fibers/epoxy/0.3 wt%
MWCNT composite plate 1 before damage was determined to be 14%.
Drilled holes and impacted areas
A hole of size 1/16 in was drilled in plate 1. The electric
potential values were measured after the hole was
drilled. These values were compared against the reference values. The difference between the electric potential values before and after drilled hole was calculated
based on equation (1). The hole is detected and located
based on the significant local variation in the distribution of the EPC, as shown in Figure 6(a). Subsequently,
another hole of size 2/16 in was drilled in plate 1. It is
observed from Figure 6(b) that the significant local variations in the distribution of the EPC reveal the locations of holes of sizes 1/16 and 2/16 in drilled in plate 1.
Other holes with different sizes were then made in plate
1. Observing Figures 6(c) and 6(d), good correspondence is observed between the significant local variations in the distribution of the EPC and holes of sizes
1/16, 2/16, 3/16, 4/16, 5/16, and 6/16 in, respectively,
drilled in plate 1. Figure 6(e) shows the effect of hole
volume on the change in electric potential. In this figure, the numbers below the curve represent the pairs of
electric potential probes. This pair of probes is
closest to the hole. A clear relationship between hole
volume and change in electric potential is observed in
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40
Structural Health Monitoring 14(1)
Figure 4. Experimental set-up to detect and locate damage due to high-velocity impact test.
Figure 5. (a) Distribution of electric potential of plate 1. The black dots, labeled 1–40, are representations of electric potential
contacts. (b) Close-up view of electrical contact points.
Figure 6(e). This reveals the capability of the technique
to determine severity of the damages.
High-velocity projectiles were impacted using a
gas gun in plate 2. Figures 7(a) and 7(b) show the
locations and values of the change in electric potential
due to the collision with high-velocity projectiles (78 J
each). By comparing Figures 7(b) and 7(c), it is
clear that impact damages 1 and 2 are detected and
located according to the sharp local variations in the
distribution of the EPC. This indicates that the technique is capable of detecting and locating impact
damages.
To explain the obtained experimental results, from
Ohm’s law, the electrical resistance R is defined by
R=
V
I
ð2Þ
where R, V , and I are electric resistance, electric potential, and electric current, respectively.
The relationship between electrical resistivity as a
material property and electrical resistance is expressed as
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R=
rl
wt
ð3Þ
41
Naghashpour and Hoa
Figure 6. Electric potential change distribution of plate 1 after drilling: (a) hole 1 (1/16 in), (b) holes 1 and 2 (1/16 and 2/16 in); (c)
holes 1–6 (1/16, 2/16, 3/16, 4/16, 5/16, and 6/16 in); (d) plate 1 (22 3 13 in2) after six drilled holes; and (e) the effect of hole volume
on the change in electric potential (data are presented as mean 6 standard deviation from three experiments).
where r, w, t, l, and R represent electrical resistivity,
width of sample, thickness of sample, distance over
which the electrical resistance is determined, and electrical resistance, respectively. Substituting equation (2)
into equation (3)
I=
V
r wtl
ð4Þ
In the case of electric potential in plate measured
using the four-probe method, constant electric
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42
Structural Health Monitoring 14(1)
Figure 7. Electric potential change distribution of plate 2 after (a) impact damage 1 (78 J) and (b) impact damages 1 and 2 (78 J
each). (c) Plate 2 (22 3 13 in2) after two impact damages.
current is injected. The electric current flowing
through the plate before damage (I1) and after damage (I2) was kept constant. Equation (4) can be written as
l
V2 r2 w22t2
=
V1 r1 wl1t
1 1
ð5Þ
where subscript numbers 1 and 2 represent before and
after damage, respectively.
If the resistivity, the distance over which the electric
potential is measured, and the thickness of plate do not
change, equation (5) can be given as
V2 w 1
=
V1 w 2
ð6Þ
If a hole (broken fibers and matrix) is made in plate,
this hole would result in a reduction in width (w2 \w1).
This reduction would cause an increase in electric
potential (V2 . V1) according to equation (6). The fraction of change in electric potential is given as
DV V2 V1 w1 w2
=
=
V1
V1
w2
ð7Þ
where w2 is smaller than w1 due to hole.
From a physical point of view, as the amount of
electric charge flowing at a given time (electric current)
is constant, the energy to push the amount of electric
charge flowing through the plate (electric potential) is
increased due to hole. As such, any discontinuity such
as hole in plate would cause an increase in electric
potential.
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Naghashpour and Hoa
Figure 8. (a) Schematic illustration of 22 3 13 in2 plate 3 impacted at three regions using drop weights with impact energies of
1–3 J. Absolute electric potential change distribution of plate 3 after (b) BVI damage 1 (1 J) and (c) BVI damages 1–3 (1–3 J).
BVI: barely visible impact.
Barely visible impact damages
Plate 3 was tested under low-velocity impact performed
using drop weights with different energy levels ranging
from 1 to 3 J. These energy levels were applied to create
barely visible impact damages (BVIDs) that cannot be
detected by visual observations. Plate 3 impacted at
three different locations with different energy levels is
schematically illustrated in Figure 8(a). Figures 8(b)
and 8(c) show the locations and values of the changes
in absolute electric potential for plate 3 due to lowvelocity impact tests. Comparing Figures 8(a) and 8(c),
good correspondence is found between the significant
local variations in absolute EPC distribution and barely
visible damage zones. This reveals that BVIDs 1–3 produced by different energy levels at different locations in
plate 3 are detected and located distinctly. From impact
damage detection and location points of view, significant change in electric potential can be taken as an indication of impact damage detection and location in the
large structures. However, complex electrical responses
due to low-velocity impact damage were observed by
many researchers for CFRPC structures.17–24,31,32 It
was shown that an impact causes electric current path
distortion, which results in a reduction in electric potential in the plane of CFRPC plate.20–22 Another explanation is that impact test may cause partial reduction in
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Structural Health Monitoring 14(1)
the thickness direction of carbon fiber/epoxy composite
laminates. This may result in fiber–fiber contacts at the
interlaminar interface and minimizing contact resistance, which may cause a reduction in electric potential,
and increasing electric current flow in interlaminar carbon fiber laminates. As such, electrical conductivity of
the laminates increases with permanent local deformation of resin caused by impact.23,24,31,32
Conclusion
A new, practical, and real-time SHM technique has
been developed to detect, locate, and quantify damages
in the large polymer composite plates made of carbon
fibers and CNT networks. In this technique, electric
current was applied through the large plate, and electric
potentials were measured. This electric potential distribution in the undamaged plate was used as a reference
map. Real-time monitoring of electric potential distribution over the surface of the plate was performed to
provide an actual map of electric potential distribution.
This map was compared against a reference map to
identify significant changes in electric potential. These
significant changes provide the ability for detection,
location, and quantification of damages and BVIDs in
the large plates.
Acknowledgements
The authors acknowledge the support from Natural Sciences
and Engineering Research Council of Canada (NSERC) and
Concordia Center for Composites (CONCOM).
Funding
This work was funded by the Natural Sciences and
Engineering Research Council of Canada (NSERC) (grant
number: RGPIN/413-2007) and Concordia Center for
Composites (CONCOM).
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